百草枯半抗原分子设计合成及表征

Synthesis and Characterization of the Hapten for Paraquat

DOI：10.3969/j.issn.1673-1689.2013.05.012

中文关键词: 百草枯 半抗原 合成 鉴定

英文关键词: paraquat hapten synthesis identification

基金项目:国家质检总局资助项目(2010QK172)

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中文摘要:

以4,4’-联吡啶和碘甲烷为起始原料,通氮气保护下于暗处经3步反应成功合成了百草枯半抗原N-甲基-N′-戊酸基-二吡啶二溴化物(简称PQ-h),产物通过LC/MS、1HNMR和IR鉴定。

英文摘要:

In this manuscript,the hapten for paraquat N-(4-carboxybutyl)-N’-methylbipyridilium(named PQ-h) was synthesized by using 4,4’-Bipyridine and iodomethane as substrate through three steps.The products was further identified through LC/MS,1HNMR and IR.This study lays the groundwork for further research of immunoassay to paraquat.

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