微波消解-ICP-AES法测定坛紫菜中重金属及近年坛紫菜金属污染调查
Determination of Porphyra haitanensis by Microwave Digestion-ICP-AES Method and Investigation Their Contaminations
DOI:10.3969/j.issn.1673-1689.2014.09.015
中文关键词: 关键字: 坛紫菜 微波消解 金属污染 ICP-AES标准曲线法
英文关键词: Porphyra haitanensis, microwave digestion, metallic pollution, ICP-AES
基金项目:
作者
单位
娄永江
宁波大学 海洋学院,浙江 宁波 315211
丁仲仲
赵一霖
郭婷婷
刘志
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中文摘要:
以东海海域某养殖场中坛紫菜为原料,采用微波消解法-ICP-AES标准曲线法对坛紫菜中铝(Al)、锌(Zn)、铜(Cu)、镉(Cd)、砷(As)、铬(Cr)和铅(Pb)7种金属元素含量进行测定。各金属元素加标回收率为95.63%~105.3%,说明微波消解-等离子电感耦合等离子体原子发射光谱法(ICP-AES)能够实现对坛紫菜重金属元素的快速精确检测。另外,监测了近5年来坛紫菜的金属污染情况,结果发现呈显著上升趋势(P
英文摘要:
A microwave digestion coupled plasma atomic emission spectroscopy(ICP-AES) method was presented for the determinations of Al, Zn, Cu, Cd, As, Cr and Pb in Porphyra haitanensis, and the samples were collected from a from in east china sea. The recovery rates of metals were between 97.8% and 104.9%, and actual applications demonstrate that this method is sensitive to achieve the determinations of metal content in Porphyra haitanensis. The results showed that an significant increasing trends were found in the metal contamination of Porphyra haitanensis during the past five years(P
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